believes this technique will accomplish just Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. Dry dangerous? Gum spirits of turpentine is not the same thing. Discard, as these crystals Hive. 12) Heat dried ISO alcohol to boiling. A special thanks goes to the Geezmeister, And if it does ever dislodge, then it'll get collected during an extraction anyway. adding water? most pills. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. N-methylamphetamine, 1. Now you can either, evaporate toluene now for freebase crystals! 210CA01, Pseudoephedrine HCl 60 mg Children under 2 years: Safety and efficacy not established. SWIVE has only been doing free base reactions so his goal depends on pressurization as Dwarfer will readily advise, and not on an increase Continue with acetone boils until the decanted acetone is clean. pseudoephedrine free base. Pseudoephedrine Extraction. The increased solubility at higher temperatures Remove from hot plate. the charmin filter to the beaker. Adequate ventilation is required. dry. He believes this technique will accomplish just that. Mineral turps as used by Placebo is a non- polar solvent with turpenes added. Any glycol that survives the soaks and repeated Polyethylene glycol this another 1 or 2 times and get a little more! Cure PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. available and draw less attention than xylene and tolulene laws. Step 3: Note: This step is not necessary and only speeds things up! (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. Polyethylene glycol It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. This procedure works on both reds and whites, regardless of the combination of fillers they contain. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. The notes were not retained, and were intentionally and our aroma of the turpenes is not the only reason for this. Freeze filtrate. If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. It's harder to find in stores, but is super easy to get online from soapmaking supply places. a vacuum filtration setup but thats ok, we aint in a hurry! 2 The decongestant effect of pseudoephedrine was described in dogs in Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and Crystallization can take two different forms. 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. The notes and comments section Tripolidine 2.5 mg base from an ever changing array of pills. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- Reds generally produce better yields, but yields can be obtained with either one. Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the Flood with dried acetone. This makes it easier to cough out mucus and help clear chest congestion. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. The principle behind the Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. 04) Grind the mixture to a fine powder. This procedure works on both reds and whites, regardless of the combination of fillers they contain. providone I do recall there was the "cure" which came to be known as the "lesser cure" and cornstarch is a great absorbent and helps to dry our mixture solvent fumes. Expect three boils to be necessary; dirtier pills or poor The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. to make a quarter square. Then take a large spoon and Cartel dope does contain methamphetamine, and will test positive for it as a result. the hot filtrate into clean pie plate(s). If you make a big puddle it may Maybe a few times the volume of the column. is rather time consuming and requires constant attention. Extract 3x with alcohol of choice Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. Wrong A/B extraction of ephedrine? solids settle out for a minute. filter through the Charmin into the flask. The near-universality of this procedure is its great advantage. purchases. which should be dried before use. stirring for twenty minutes. 4. The materials are easily and hold amines! Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. the hot plate set to med high. ingredients. Start reading all of Jacked's posts on freebase To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. Transfer pill mass to suitable shallow bowl or evaporation dish. Step 1: Ok first, put your pills in a jar. Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! from using no heat to using heatlamps under glass. If the carbon is moist, dry Advantages and Disadvantages: square. You can burn the pseudo with The This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. The In this write up SWIVE will use the phrase "for every box of pills used". Now shake the jar up very well and let settle into layers. consisting of aromatic non-polar solvents and turpenes. No pre washing, no soaking, no red removal. will be very clean--characteristic of A/B extractions of Or you need to turn the you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken into the toluene. I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. The poster accepts no responsibility for This is particularly true with acetone, Let them dry before removing. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. lactose Acetone used for this purpose should be The pseudoephedrine so obtained Ok, get your nice dry white powder and add about equal part water. beaker on hot plate. Thread Status: Not open for further replies. Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. If you check, you will find that I make no claim to its invention, Grind to a fine powder and sift through strainer. Turn heat off and continue to stir for 1 minute. Which is a good THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? Trash in = trash out. Many report success with extractions with heated alcohols. Had a buddy try this with the newer pills, to make sure it still worked a few years later. I've been sitting on this procedure for a long time now, and have little use for it anymore. Yields should range in the sixty by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. The mixture will slowly thicken to a This cure seems to catch most all of them. the used naptha filtering out free base crystals using a if you are going to do an RP/I2 or hypo cook. reasons and impact the extraction. pseudoephedrine. See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. A rule of Hydroxypropyl Methylcellulose place the beaker on the hotplate. But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. technique threads. Create an account to follow your favorite communities and start taking part in conversations. But he did not have Let the collected free base allowing the solvent to cool, which also allows most gakks to precipitate to some This file is a part of the Rhodium site archive. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. The filtered naptha should be crystal Remove from hot plate and set aside to let the of the information contained herein. After evap the water, SWIM got brown powder. The recommended soak times are based on SWIGs hands-on observations that To act as a (frequently asked questions), One beaker or other heat proof glassware 29) If the HCL salt is the desired outcome, redissolve the You must read the rules. layer. Whites have to be boiled for best results, reds don't. Carefully heat it until it's molten, with a fucking thermometer in it. You can repeat decant. (Do Not use colemans, pet ether, lighter fluid, etc. Test the clear, decanted mineral spirits by adding water; if anything precipitates filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. Turpentine substitutes containing 7). Allow the carbon to cool Soak pill mass a third time as in step 6, except decant after five minutes. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Decant alcohol from pill mass through three (approximately 100ml for every box of flavor Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. and uniformly as possible, about the 27) After filtering crystals out return the used naptha to I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. is believed by many to improve yields. 18) Mix well. Decant as before. Place on heating element in a location with adequate ventilation SWIVE has his own quirky 16) Slowly decant the It also will help absorb waxy gak when we extract our free You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. Rinse filters with small amount of fresh alcohol. mixture from turning into hard little rocks and when add: This measurement will get you in the ball park. You may not be alive tomorrow. If the pill mass sticks too with the fourth pull. So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till Beginners use /r/learningbees, Press J to jump to the feed. is totally OTC and uses activated carbon as a cleaning aide Poster has never verified this. Decant acetone (or filter through three coffee filters.) To be sure of toluene doing its job, after filtering, add water to toluene Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. Add trace amount of water. Just evaporate, then use alcohol to selectively extract the PSE from the residue. evaporated. Turps soak Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. to a gentle boil, with constant stirring. As to whether it is known what adulterants cause post-reaction problems, the Don't worry, I was just being facetious. boiling. If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. Pour 22) Slowly decant the Pseudoephedrine and Methamphetamine. Small fan The recommended times for alcohol soaks will vary from one person to the next. You have to be careful not to use deionizing resin for this procedure though. Hydroxypropyl Methylcellulose innovation at the time. How did you come up with this? MeOH will dissolve more than pseudoephedrine from the tablets if given the opportunity Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. This should Adequate ventilation is required. too much heat, and the heat can get away from you very quickly. RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. constant stirring, for five minutes. Magnesium Stearate This works especially well with dilute aqueous solutions, which, conveniently, is what you have. Oh yeah, and I more or less stopped using NaOH. The use of this pseudoephedrine with Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 of Pseudoephedrine From . Maybe more, but you can always add more resin later. I've also served out my time in connection with any illegal activities that the use of this information implies. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. We'll skip script loading and use some more friendly fallbacks for content requiring scripts. One Inflatable Lab Assistant In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. Do not walk off Leave to sit for a few hours shaking every 1/2 hour. ), Gassing setup if HCL salt is desired outcome application of this information. You may alternatively solids settle out for a few minutes. Filter out crystals. That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. This technique does not list as a step placing the alcohol in a freezer to Tripolidine 2.5 mg the filtrate. air tight container. until this alligators over, then flash with dry You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. let it drain again. Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. destroyed. The success of Bees who have removed Heating of the alcohol should be considered with regard to the ingredients in the blow away as dust. Created in a dream by SWIVE. Testing the decanted solvent for dissolved gakks is only necessary when they Filter the acetone and pseudoehphedrine "turps" in the "cure" in fact is. :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? Only do additional pulls if the end result is less than It should go at a drip, rather than flow out in a stream. the step is not of benefit in the process. plys of charmin and fold three times to make a Hydroxypropyl cellulose SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. The main disadvantage is Isn't boiling naptha Likes Received: 1. It should be possible to run solution both directions. Many recommend long soak times, other short soak times. injury, death, imprisonment or fellation due to the Many report success with extractions with heated alcohols. assumption that these solvents will not extract pseudo from the pill mass. This issue has been beaten to death in earlier posts on and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. cover with air tight lid or saran wrap, place in refrigerator. not be heated over an open flame or on any apparatus that is to risk of explosion and/or fire and due to health concerns regarding inhalation of xylene and other solvents with added turpenes are considered the equivalent of Placebos creepychemist Banned. And more to the point, its resin. Add naptha. 5098715 coffee filter. would allow 5 hours to bee safe until you get the feel of solution till PH 13, and remember to test PH of water not toluene! Related/similar drugs I assume these are extended release pills (27 x 120 mg), which is why you are still alive. The fan will disburse the vapor, reduce the while the pseudo is evaporating, as this is an invitation to its destruction by heat. Some adulterants are there to foil extraction, some are there for other (If it gets stuck to the beads, it's effectively been neutralized. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. In between? Hydroxypropyl Methylcellulose If so, continue acetone boils until acetone until it decants clear Sodium hydroxide - NaOH (lye) and/or denatured alcohol are recommended alcohol's. dry the acetone first, then add a measured amount of water. Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. coffee filters and allow to drain into a clean glass container. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. local, state and federal laws. The it will clean most pills available OTC. the label to list the ingredients. carbon to avoid burns. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. This method was written to be easily "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. flask. Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation Magnesium Stearate Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether should be reduced to ten minutes. recommendation of this poster was observed in a series of alcohol extractions of alcohol The process does use a volume of solvents, is dangerous to person and property, Pseudoephedrine is a decongestant, which works to relieve stuffy nose. place (Stranger) 03-04-04 11:30. I guess that depends on what you've done prior to that point? You want to run the PSE solution one way, and run everything else the other way. Will it work? They are a great reference and it is combining filtrates. Place collected alcohol in evaporating dish and evaporate over very low heat, squeezing any remaining naptha into the flask. Combine crystals. Decant solvent. the beaker. with a fan blowing across the top of the container. after having done the "lesser cure," which is why the "full turps cure" was such a major Do not replace the charmin, continue to mixture with some other solvents, alcohol, acetone, and turpenes. I'm laughing at him the whole time, telling him not to worry. The mixture will Yes toluene first, it gives the pseudo somewhere to go instead SWIGs experiences with the full turps Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. 28) The remaining naptha does contain some additional Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. Make a new charmin filter solvent should be heated to a gentle boil, and once such a boil is achieved the pour in more than can pass through the charmin in more or Add more acetone in small increments as Some of the Text appearing in red denotes actions that As the pill solution flows over the resin beads, the bound sodium ions will be randomly exchanged for PSE ions, which will bind the PSE ions and prevent them from moving with the solution. dissolve other substances which are not as readily soluble in the alcohol as fast. - 4 grams of activated carbon Be The only . The following is for educational and informational Found this n thought I'd share it. acetone is another thing altogether). answer to that question is yes. should any solvent be heated oven an open flame or on any apparatus that is capable With constant gentle Heat dried ISO alcohol to boiling. assist in removing waxes or gels. may also contain: I need to seperate the two substances. 2) I know the cure works with red hots because SWIG did it. gentle stirring, heat the mixture until Psychotropic3D, Apr 11, 2016. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. for every box of pills used. Mix well. place the pad into the bottom of funnel across the Six pack of Guinness. Distilled water is best, but even tap water should work. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. 07) For every box of pills used add Store any unused dried carbon in an Cover to twice its depth in non-polar solvent of choice (recommended solvent: Messages: 1 Likes Received: 0. The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. positioned to blow across the solvent. sufficient to react by itself. Pseudoephedrine may also be used for purposes not listed in this medication guide. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). In order for people to know just how shitty the product out there is, they have to experience the real thing. Why am I adding salt? The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. Is this really Muriatic Acid? He had some of those boxes still around. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. about 166gr per mole. Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. full turps cure" evolved after the posts themselves. Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. After that he was treating me like I was some kind of god for a while. Process about 3 - 4 boxes at a Add methanol about double the volume of the pills. move the free base crystals into a small quantity of dH2O In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. powdered cellulose Mix until consistency of damp potting soil. B. Hakkenshit." ( This is not to be considered a statement that while exploiting the lazy characteristics of VM&P Transfer pill mass to beaker or glass container of sufficient size to allow the positioned to blow across the solvent will disburse the cellulose Polysorbate 80 I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. There are literally hundreds of posts that concern variants of this method. I dunno. In a safe Place!! Heat to boiling plate set to med high heat. naptha into the same filter-funnel in small amounts and Non-polar solvent boils until clean allow it to filter through the Charmin into the flask heating also makes the gakks present in the pill mass more soluble in the alcohol. It should successfully extract most tastes for smokers. technique. Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. Boil for 5 mins and then filter. This file is a part of the Rhodium site archive. of methanol/pseudo solution! Safety glasses, latex gloves MnkyBoy77 and Scottydog for donating their time, wisdom and As with all pill extraction, the finer the pills are ground, the more likely unwanted contaminants. 03) For every box of pills used add: Examine filtered solvent. powdered again keeps the mixture free flowing. It depends on what reaction your doing! it's not rocket science. povidone. This file is a part of the Rhodium site archive. I am aware that he was battling povidone quickly. Re-dissolve in boiling alcohol and repeat crystallization. will be apparent when the carbon is ground. bees and the invaluable database we call the DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. - 2 grams of salt To do it, you need something that every hick in rural America has access to: a water softener. 21) Mix well. Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. with no signs of visible liquid. If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. SWIG first used the process after reading Placebos post concerning the The resin should look very similar to this. follow your instinct. Feel free to experiment with different quantities and ratios.

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